• 专利标题:   Method for preparing graphene-modified lithium ion battery cathode material, involves keeping mixed gas of hydrogen and methane for certain period of time, then closing system and cooling sample to room temperature to obtain final product.
  • 专利号:   CN108682859-A
  • 发明人:   YANG C, ZHOU P, ZHAO D
  • 专利权人:   FUJIAN XIANGFENGHUA NEW ENERGY MATERIAL
  • 国际专利分类:   H01M004/62
  • 专利详细信息:   CN108682859-A 19 Oct 2018 H01M-004/62 201878 Pages: 9 Chinese
  • 申请详细信息:   CN108682859-A CN10379356 25 Apr 2018
  • 优先权号:   CN10379356

▎ 摘  要

NOVELTY - The method involves weighing certain amount of silicon-oxide powder, putting the silicon-oxide powder into a tubular furnace, and heating silicon-oxide powder to 1000 degrees C for a period of time to carry out the disproportionation reaction under vacuum conditions. The micron level copper powder is ultrasonicated for period of time using acetone solution, and after drying, the micron level copper powder is mixed with the silicon-oxide powder. The mixture is placed in a high energy ball mill for grinding. The ground precursor material is taken out, and poured into a crucible, and then crucible is placed in a tubular furnace, and temperature is raised under the argon atmosphere. An argon gas valve is closed, when the temperature reaches 1050 degrees C. The mixed gas of hydrogen and methane is filled according to proportion in a quartz tube and kept for certain period of time, then temperature control system is closed and sample is naturally cooled to room temperature to obtain the final product. USE - Method for preparing graphene-modified lithium ion battery cathode material. ADVANTAGE - The graphene and the copper particles in the prepared material contains good electrical conductivity and good reversible cycle performance, and the conductivity of the two materials is improved by the addition of the two materials, the other electrochemical properties of the material is improved greatly. DESCRIPTION OF DRAWING(S) - The drawing shows a graphical diagram showing the charge and discharge capacity-voltage. (Drawing includes non-English language text)