• 专利标题:   Nitrogen-sulfur double-doped porous carbon material catalyst comprises porous carbon material includes cysteine as nitrogen-sulfur source and glucose as carbon source.
  • 专利号:   CN113649044-A
  • 发明人:   LI J, WANG Q, JIN Z, BEI K, HUANG X, LIU J, ZHENG X, ZHAO M, AN N, LIU R
  • 专利权人:   UNIV WENZHOU
  • 国际专利分类:   A62D101/20, A62D003/38, B01J027/24, B01J035/10, B01J037/10
  • 专利详细信息:   CN113649044-A 16 Nov 2021 B01J-027/24 202237 Chinese
  • 申请详细信息:   CN113649044-A CN10944217 17 Aug 2021
  • 优先权号:   CN10944217

▎ 摘  要

NOVELTY - Nitrogen-sulfur double-doped porous carbon material catalyst is claimed. The porous carbon material includes nitrogen-sulfur source and carbon source in a mass ratio of 1-50 wt.%, the carbon source is glucose, and the nitrogen-sulfur source is cysteine. USE - Used as nitrogen-sulfur double-doped porous carbon material catalyst. ADVANTAGE - The nitrogen-sulfur double-doped porous carbon material catalyst: has excellent catalytic performance; and exhibits synergistic effect which promotes the adsorption and catalytic degradation of antibiotic organic pollutants; and co-doping of nitrogen and sulfur not only ensures the catalytic stability of the catalyst. The method: utilizes available cheap and easily available raw materials; is environmentally friendly and pollution-free and has low production cost. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing nitrogen-sulfur double-doped porous carbon material catalyst comprising (i) taking certain amount of carbon source, nitrogen source and sulfur source, mixing and dispersing them in an aqueous solution, then transferring to a hydrothermal reactor container, raising the temperature to a certain temperature and keeping for certain period of time to obtain carbon material containing carbon, nitrogen and sulfur, (ii) introducing synthesized carbon material containing carbon, nitrogen and sulfur into a quartz glass container, adding inert gas as a protective gas, calcining at a high temperature for a certain period of time, grinding and pulverizing, natural cooling to obtain nitrogen-sulfur double-doped carbonized material, (iii) adding synthesized nitrogen-sulfur double-doped carbonized material into a customized crucible, adding certain proportion of sodium hydroxide solution and anhydrous ethanol, stirring evenly, uniformly transferring to an oven for drying at a certain temperature, then transferring to a high temperature tubular furnace, introducing inert gas as a protective gas, calcining at high temperature for a certain period of time, and natural cooling to obtain final product.