• 专利标题:   Preparing graphene from graphite used in coatings, comprises obtaining mixture containing graphite, ammonium thiosulfate, urea salt, silane and hydrogen peroxide, obtaining homogeneous solution by sonicating and irradiating stock solution.
  • 专利号:   IN201621014972-A
  • 发明人:   MALLICK S, BOHM S, NEMALA S S
  • 专利权人:   INDIAN INST TECHNOLOGY BOMBAY
  • 国际专利分类:   C01B032/192, C01B032/198
  • 专利详细信息:   IN201621014972-A 03 Nov 2017 C01B-032/192 201778 Pages: 16 English
  • 申请详细信息:   IN201621014972-A IN21014972 29 Apr 2016
  • 优先权号:   IN21014972

▎ 摘  要

NOVELTY - Preparing graphene from graphite, comprises: obtaining a mixture consisting of a predefined quantity of graphite, ammonium thiosulfate, urea salt, silane and hydrogen peroxide respectively; obtaining a homogeneous solution by sonicating the mixture for a predefined period; obtaining a stock solution by performing a reflux of the homogeneous solution for a predefined time; and performing an irradiation of the stock solution in a microwave furnace at a predefined power for a predefined period, where graphene is obtained through exfoliation of graphite. USE - The process is useful for preparing graphene from graphite (claimed) which is useful in photovoltaics, coatings, energy storage, heat transfer applications in power plants, bitumen systems for transport applications. ADVANTAGE - The process: is easy, cost-effective and eco-friendly for bulk production of exfoliated graphene, synthesize graphene at a faster rate (within 180 seconds) which is amenable for industrial applications; does not require any hazardous acids or other toxic chemicals; allows control of the defect concentration in graphene based on microwave conditions and the chemicals used.