• 专利标题:   Preparing low viscosity epoxy resin comprises e.g. sending graphene into modifier to improve ultrasonic treatment, washing with water, drying, adding bisphenol A epoxy resin to acetone solvent, adding modified graphene, N-methylol acrylamide and ammonium persulfate, pre-mixing, and stirring.
  • 专利号:   CN114539698-A
  • 发明人:   LIU X, SUN W, DONG N, WANG D, WU D, YIN X, XIE X, ZHANG F, XING X
  • 专利权人:   SHANDONG QICHUANG PETROCHEM ENG CO LTD
  • 国际专利分类:   C08K013/06, C08K003/04, C08K003/36, C08K005/3492, C08K007/10, C08K009/06, C08L033/00, C08L005/08, C08L063/02, C08L071/02
  • 专利详细信息:   CN114539698-A 27 May 2022 C08L-033/00 202273 Chinese
  • 申请详细信息:   CN114539698-A CN10318719 29 Mar 2022
  • 优先权号:   CN10318719

▎ 摘  要

NOVELTY - Preparing low viscosity epoxy resin comprises (i) sending graphene into a modifier to improve the ultrasonic treatment, finishing the ultrasonic treatment, washing with water, and drying to obtain modified graphene, (ii) adding 10-30 pts. wt. bisphenol A epoxy resin to 45-55 pts. wt. acetone solvent, adding 1-5 pts. wt. modified graphene, 1-2 pts. wt. N-methylol acrylamide and 0.5-0.9 pts. wt. ammonium persulfate, and pre-mixing to obtain a premix, (iii) adding the premix into a modified emulsion in a weight ratio of 1:3, stirring, and processing to obtain resin, and (iv) sending the resin at 45-55°C, and allowing to stand for 15-25 minutes to obtain the product. USE - The method is useful for preparing low viscosity epoxy resin. ADVANTAGE - The method: utilizes the graphene for modification, and a modified emulsion for coordinate the modification; enhances the bonding strength of bisphenol A epoxy resin; and improves the adhesion of the product to the substrate.