• 专利标题:   Method for electrochemical detection of acetaminophen, involves preparing poly-3.4-dioxoethylenethiophene/graphene oxide/glassy carbon electrode by mixing pure 3,4-ethylenedioxythiophene monomer in graphene oxide ultrasonically.
  • 专利号:   CN103604858-A, CN103604858-B
  • 发明人:   HAN Z, HAO Q, LEI W, XIA M, WANG F, SI W
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   G01N027/30, G01N027/48
  • 专利详细信息:   CN103604858-A 26 Feb 2014 G01N-027/48 201432 Pages: 8 Chinese
  • 申请详细信息:   CN103604858-A CN10584763 20 Nov 2013
  • 优先权号:   CN10584763

▎ 摘  要

NOVELTY - An acetaminophen electrochemical detection method involves preparing poly-3.4-dioxoethylenethiophene/graphene oxide/glassy carbon electrode (PEDOT/GO/GC electrode) by mixing pure 3,4 ethylenedioxythiophene monomer in graphene oxide ultrasonically for half an hour to obtain mixed solution. The glassy carbon electrode is placed in a mixed solution to obtain PEDOT/GO/GC electrode. The electrode is placed in a buffer solution, followed by adding acetaminophen, and using the electrode to detect acetaminophen electrochemical response. USE - Method for electrochemical detection of acetaminophen. ADVANTAGE - The method enables electrochemical detection of acetaminophen with better repeatability and high stability in a rapid manner. DETAILED DESCRIPTION - An acetaminophen electrochemical detection method involves preparing poly-3.4-dioxoethylenethiophene/graphene oxide/glassy carbon electrode (PEDOT/GO/GC electrode) by mixing pure 3,4 ethylenedioxythiophene monomer in graphene oxide ultrasonically for half an hour to obtain mixed solution. The glassy carbon electrode is placed in a mixed solution at a potential range of 0.2-1.2 V for cyclic voltammetry polymerization of 5-30 laps, and cyclic volt-ampere scanning speed at 100 mV/second to obtain PEDOT/GO/GC electrode. The electrode is placed in a buffer solution with pH of 2.8-7.0, followed by adding acetaminophen, using cyclic voltammetry scanning rate of 100-300 mV/s and the electrode to detect acetaminophen electrochemical response.