• 专利标题:   Selective water blocking agent preparation involves mixing graphene oxide with N,N-dimethylformamide and ultrasonically dispersing to obtain graphene oxide dispersion, and then mixing with organic amine and adding dicyclohexylcarbimide.
  • 专利号:   CN108949130-A
  • 发明人:   PEI W, LIU X, ZHU D
  • 专利权人:   PEI W
  • 国际专利分类:   C09K008/508, C08F220/56, C08F220/58, C08F226/02
  • 专利详细信息:   CN108949130-A 07 Dec 2018 C09K-008/508 201914 Pages: 7 Chinese
  • 申请详细信息:   CN108949130-A CN10817176 24 Jul 2018
  • 优先权号:   CN10817176

▎ 摘  要

NOVELTY - Selective water blocking agent preparation involves mixing graphene oxide with N,N-dimethylformamide in a mass ratio of 1:200-1:400 and ultrasonically dispersing to obtain a graphene oxide dispersion, and then mixing with organic amine and adding dicyclohexylcarbimide with stirring. The supernatant is removed to obtain pre-modified oxidation graphene mixture, which is filtered, washed, and dried to obtain pre-modified graphene oxide. The obtained pre-modified graphene oxide is mixed with an organic solvent in a mass ratio of 1:20-1:30, and then mixed with the pre-modified graphene oxide and water with stirring to obtain modified graphene oxide. The acrylamide and methyl silicic acid are mixed in a mass ratio of 1.8:1.0-2.0:1.0, and then added to 2-acrylamide-2-methylpropanesulfonic acid with stirring to obtain pretreatment mixture. USE - Method for preparing selective water blocking agent. ADVANTAGE - The method prepares the selective water blocking agent in a simple, cost-effective and eco-friendly manner with excellent selective permeability and water blocking performance. DETAILED DESCRIPTION - The obtained pretreatment mixture is mixed with silane coupling agent in a mass ratio of 80:1-100:1, and then added to modified graphene oxide, catalyst and epoxy soybean oil with stirring to prepare a mixture. The prepared mixture is pumped, filtered, washed, dried, and pulverized to obtain the selective water blocking agent.