• 专利标题:   Preparation of single-crystal graphene comprises affixing graphite crystal to base area, coating layer with nickel and/or copper alloys, heating, annealing, cooling, immersing in iron chloride solution and removing metal layer and carbon.
  • 专利号:   CN103074678-A
  • 发明人:   LI X, LIN S
  • 专利权人:   HANGZHOU GELANFENG NANO TECHNOLOGY CO LT
  • 国际专利分类:   C30B029/02, C30B033/02, C30B033/10
  • 专利详细信息:   CN103074678-A 01 May 2013 C30B-029/02 201367 Pages: 6 Chinese
  • 申请详细信息:   CN103074678-A CN10042925 04 Feb 2013
  • 优先权号:   CN10042925

▎ 摘  要

NOVELTY - Preparation of single-crystal graphene comprises affixing graphite crystal to base area using tear tape to obtain seed layer, coating layer with nickel alloy and/or copper alloy with thickness of 10-20 mu m, covering with carbon source, heating in furnace to 200-400 degrees C with maintained pressure of 1.01x 105 Pa, reacting under protective atmosphere of argon, nitrogen, helium or neon gases, annealing for 100 seconds-1 hour, cooling to room temperature, immersing in iron chloride solution and removing metal layer and carbon source. USE - Method for preparing single-crystal graphene (claimed).