• 专利标题:   In-line preparation of cubic copper oxide/graphene aerogel composite material involves pouring oxidized graphene dispersion into autoclave liner, adding pretreated copper mesh performing hydrothermal reaction, quenching and freeze-drying.
  • 专利号:   CN106683909-A, CN106683909-B
  • 发明人:   LU Y, LUO Y, CENG F, LUO R, YU Q
  • 专利权人:   UNIV XINYANG NORMAL
  • 国际专利分类:   B01J021/18, B01J023/72, B82Y030/00, H01G011/36, H01G011/46, H01G011/86, H01M010/0525, H01M004/36, H01M004/48, H01M004/62
  • 专利详细信息:   CN106683909-A 17 May 2017 H01G-011/86 201740 Pages: 10 Chinese
  • 申请详细信息:   CN106683909-A CN10049118 23 Jan 2017
  • 优先权号:   CN10049118

▎ 摘  要

NOVELTY - An in-line preparation of cubic copper oxide/graphene aerogel composite material, involves (i) placing copper mesh into hydrochloric acid, ultrasonically cleaning with anhydrous ethanol and deionized water, and drying, (ii) ultrasonically dispersing graphene oxide in deionized water to obtain an oxidized graphene dispersion, (iii) pouring the oxidized graphene dispersion into an autoclave liner, then adding the obtained copper mesh, performing hydrothermal reaction, (iv) taking out the product, quenching and freeze-drying at -30 degrees C to -50 degrees C for 12-48 hours. USE - In-line preparation of cubic copper oxide/graphene aerogel composite material (claimed). DETAILED DESCRIPTION - An in-line preparation of cubic copper oxide/graphene aerogel composite material, involves (i) placing copper mesh into hydrochloric acid, ultrasonically cleaning with anhydrous ethanol and deionized water, and drying, (ii) ultrasonically dispersing graphene oxide in deionized water to obtain an oxidized graphene dispersion having a concentration of 1-5 mg/mL, (iii) pouring the oxidized graphene dispersion into an autoclave liner, then adding the obtained copper mesh into the autoclave liner, performing hydrothermal reaction at 120-200 degrees C for 6-15 hours, (iv) taking out the product, quenching and freeze-drying at -30 degrees C to -50 degrees C for 12-48 hours under the vacuum degree of 10-30 Pa to obtain copper oxide/graphene aerogel composite material.