• 专利标题:   Preparation of tungsten sulfide/titanium dioxide/nitrogen-doped graphene nanocomposite material by dispersing graphene oxide in water, adding e.g. aniline, sodium lauryl sulfate and thioacetamide, reacting and drying.
  • 专利号:   CN112216833-A
  • 发明人:   ZHANG Z, SHU J, ZHANG L, GAO W
  • 专利权人:   UNIV YULIN
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/48, H01M004/58, H01M004/583
  • 专利详细信息:   CN112216833-A 12 Jan 2021 H01M-004/36 202119 Pages: 5 Chinese
  • 申请详细信息:   CN112216833-A CN11256824 11 Nov 2020
  • 优先权号:   CN11256824

▎ 摘  要

NOVELTY - Preparation of tungsten sulfide/titanium dioxide/nitrogen-doped graphene nanocomposite material comprises dispersing graphene oxide uniformly in water by ultrasonic mixing, adding aniline and sodium lauryl sulfate, sonicating for 20-40 minutes, adding ammonium persulfate hydrochloric acid solution, stirring under ice bath for 12-24 hours, adding tungsten chloride, thioacetamide and titanium dioxide, mixing, adding to hydrothermal kettle under airtight conditions at 220-260 degrees C, reacting for 10-24 hours, washing precipitates repeatedly with deionized water and ethanol, and vacuum drying. USE - The method is used for preparing tungsten sulfide/titanium dioxide/nitrogen-doped graphene nanocomposite material. ADVANTAGE - Aniline is used to form polyaniline beads to expand graphene sheet structure to increase specific surface area of material. The preparation method is simple and low in cost. The nanocomposite material has two-dimensional flake structure.