• 专利标题:   Preparation of graphene oxide doped mesoporous silicon film for selectively adsorbing rare earth elements, involves preparing nanocrystalline cellulose, dispersing, reacting with glucose, graphene oxide, tetraethyl silicate, sulfuric acid.
  • 专利号:   CN108325507-A
  • 发明人:   LIU E, ZHAG F, YAN Y
  • 专利权人:   UNIV JIANGSU
  • 国际专利分类:   B01J020/24, B01J020/28, B01J020/30, C22B003/24, C22B059/00
  • 专利详细信息:   CN108325507-A 27 Jul 2018 B01J-020/24 201858 Pages: 12 Chinese
  • 申请详细信息:   CN108325507-A CN10279035 30 Mar 2018
  • 优先权号:   CN10279035

▎ 摘  要

NOVELTY - The preparation of graphene oxide doped mesoporous silicon film, involves (1) preparing nanocrystalline cellulose, (2) ultrasonically dispersing nanocrystalline cellulose, adding solution of glucose and graphene oxide, mixing thoroughly, dripping diethylphosphorylethyltriethoxysilane and tetraethyl silicate, respectively, stirring, pouring into Teflon (RTM: PTFE) tray and drying to obtain mesoporous silicon film (A), (3) placing mesoporous silicon film (A) in sulfuric acid solution to remove template molecule nanocrystalline cellulose to obtain mesoporous silicon film (B), (4) reacting mesoporous silicon film (B) in concentrated hydrochloric acid to obtain mesoporous silicon film (C), (5) alternately washing mesoporous silicon film (C) with distilled water and absolute ethanol and drying. USE - Preparation of graphene oxide doped mesoporous silicon film for selectively adsorbing rare earth elements (claimed). ADVANTAGE - The method enables preparation of graphene oxide doped mesoporous silicon film ensuring excellent adsorption performance by simple, easy and environmentally-friendly process.