• 专利标题:   Preparation of graphene/chitosan porous sponge material involves adding graphene oxide solution to chitosan solution, adding glutaraldehyde to graphene/chitosan mixture solution, crosslinking and freezing mixture.
  • 专利号:   CN103464114-A, CN103464114-B
  • 发明人:   TANG X, TIAN M, GUO X, QU L
  • 专利权人:   UNIV QINGDAO
  • 国际专利分类:   B01J020/24, B01J020/28, B01J020/30
  • 专利详细信息:   CN103464114-A 25 Dec 2013 B01J-020/24 201417 Pages: 6 Chinese
  • 申请详细信息:   CN103464114-A CN10434295 23 Sep 2013
  • 优先权号:   CN10434295

▎ 摘  要

NOVELTY - A graphene oxide solution having concentration of 2-5 %mass is added to a chitosan solution having concentration of 2-4 %mass and stirred, to obtain homogeneous mixture of graphene/chitosan mixture solution having graphene oxide content of 6-30%. Glutaraldehyde is slowly added to graphene/chitosan mixture solution, stirred and crosslinked at 60-100 degrees C for 1-4 hours, frozen in vacuum freeze drier, and freeze-dried for 24 hours or more, to obtain graphene/chitosan porous sponge material having three-dimensional structure. USE - Preparation of graphene/chitosan porous sponge material (claimed). ADVANTAGE - The method enables preparation of graphene/chitosan porous sponge material having high porosity, absorption rate and stability.