• 专利标题:   Preparing oxygen-containing functionalized graphene useful in field of electrochemical energy storage/conversion, comprises mixing strong oxidizing compound and graphite, placing in sulfuric acid, filtering, stripping and heat treating.
  • 专利号:   CN110092370-A
  • 发明人:   XIA H, LUO D, XU J, YANG M, GUO Q
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   C01B032/182, C01B032/198
  • 专利详细信息:   CN110092370-A 06 Aug 2019 C01B-032/182 201978 Pages: 6 Chinese
  • 申请详细信息:   CN110092370-A CN10095128 31 Jan 2018
  • 优先权号:   CN10095128

▎ 摘  要

NOVELTY - Preparing oxygen-containing functionalized graphene comprises (i) mixing strong oxidizing compound and graphite in a mass ratio of 1:2-10:1, placing in concentrated sulfuric acid, stirring in an ice bath for 3-24 hours, adding water, stirring at 20-40 degrees C for 2-16 hours, then stirring at 75-95 degrees C for 2-16 hours, adding hydrogen peroxide, repeatedly filtering using 5% dilute hydrochloric acid solution when solution turns golden yellow and drying to obtain solid graphite oxide; (ii) stripping the solid graphite oxide at 250-350 degrees C in air atmosphere for 10-30 minutes to obtain oxygen-containing functionalized graphene oxide; and (iii) heat treating the oxygen-containing functionalized graphene oxide at 500-1000 degrees C for 1-6 hours in an argon atmosphere. USE - The graphene is useful in field of electrochemical energy storage/conversion. ADVANTAGE - The graphene has high surface area and mesoporous structure.