• 专利标题:   Preparation of highly thermally conductive flexible graphene film, involves ultrasonically dispersing graphene powder in deionized water, to obtain slurry, adding aqueous ammonia and stirring, and adding hydroxylamine hydrochloride.
  • 专利号:   CN106495133-A
  • 发明人:   LU B, LI P
  • 专利权人:   JIAXING ZHONGYI CARBON TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106495133-A 15 Mar 2017 C01B-032/184 201733 Pages: 6 Chinese
  • 申请详细信息:   CN106495133-A CN10985554 09 Nov 2016
  • 优先权号:   CN10985554

▎ 摘  要

NOVELTY - Preparation of highly thermally conductive flexible graphene film, involves (i) dispersing 0.6-3.2 wt.% graphene powder in 96.8-99.4 wt.% deionized water, stirring and ultrasonically processing for evenly distributing to obtain slurry, (ii) adding aqueous ammonia and stirring for 0.5-1 hour, adjusting the pH of slurry to 9-11, (iii) adding a reducing agent hydroxylamine hydrochloride to reduce the graphene oxide, (iv) coating the reduced graphene paste on a dry film, and stripping, (v) carrying out high-temperature hot-pressing and sintering on reduced graphene film to graphitize. USE - Preparation of highly thermally conductive flexible graphene film (claimed). DETAILED DESCRIPTION - Preparation of highly thermally conductive flexible graphene film, involves (i) dispersing 0.6-3.2 wt.% graphene powder in 96.8-99.4 wt.% deionized water, stirring and ultrasonically processing for evenly distributing to obtain slurry, (ii) adding aqueous ammonia and stirring for 0.5-1 hour, adjusting the pH of the slurry to 9 to 11, (iii) adding a reducing agent hydroxylamine hydrochloride to reduce the graphene oxide, (iv) coating the reduced graphene paste on a dry film, and stripping, (v) carrying out high-temperature hot-pressing and sintering on reduced graphene film to graphitize, and obtaining highly thermally conductive flexible graphene film.