• 专利标题:   Preparation method of nitrogen-chlorine co-doped graphene involves graphite material as working electrode, platinum as counter electrode in mixed solution of ammonium nitrate and ammonium chloride, using constant voltage technology to electrochemical graphite.
  • 专利号:   CN114560462-A
  • 发明人:   XU C, LI Q, ZHENG H
  • 专利权人:   UNIV JINAN
  • 国际专利分类:   C01B032/19, C01B032/194
  • 专利详细信息:   CN114560462-A 31 May 2022 C01B-032/19 202259 Chinese
  • 申请详细信息:   CN114560462-A CN10183941 28 Feb 2022
  • 优先权号:   CN10183941

▎ 摘  要

NOVELTY - The method involves using graphite material as the working electrode, and the platinum is used as the counter electrode. In the mixed solution of ammonium nitrate and ammonium chloride, the electrochemical exfoliation of the graphite material is carried out by using a constant voltage technique. Washing, sonicating and standing the solution after electrochemical stripping. The freeze-drying treatment is performed on the supernatant to obtain nitrogen-chlorine co-doped graphene. USE - Preparation method of nitrogen-chlorine co-doped graphite used as electrode material in wearable electronic product and other devices. ADVANTAGE - The method enables to prepare nitrogen-chlorine-co-doped graphene, which has large edge size, which is good for obtaining more excellent charge storage performance. The method uses conventional chemical raw material, fast, direct, preparation yield, low raw material cost is low, preparation method has expandability, convenient for mass production, and the product has larger edge size. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic view of scanning electron microscope picture of the prepared nitrogen-chlorine co-doped graphene.