• 专利标题:   Vibration and delamination of graphene using alternating electric field by drying graphite powder and grinding medium ceramic and medium metal microspheres, placing in grinding cavity, applying alternating electric field, and grinding.
  • 专利号:   CN107416810-A
  • 发明人:   CHEN Q, ZENG J, CHEN B
  • 专利权人:   CHENGDU NEW KELI CHEM SCI CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN107416810-A 01 Dec 2017 C01B-032/19 201801 Pages: 8 Chinese
  • 申请详细信息:   CN107416810-A CN10461871 19 Jun 2017
  • 优先权号:   CN10461871

▎ 摘  要

NOVELTY - Vibration and delamination of graphene using alternating electric field comprises cleaning graphite powder, removing impurities, drying under argon protection, and standing; washing and drying grinding medium ceramic microspheres, and washing and drying grinding medium metal microspheres; and placing graphite powder, ceramic microspheres and metal microspheres at mass ratio of 1:1-5:1-5 in grinding cavity, vibrating and colliding metal microspheres by applying alternating electric field to drive ceramic microspheres and graphite to make disorder movement, and grinding for 0.5-1 hour. USE - Method for vibration and delamination of graphene using alternating electric field (claimed). ADVANTAGE - The method realizes controllable mechanical force, and has high yield. DETAILED DESCRIPTION - Vibration and delamination of graphene using alternating electric field comprises cleaning graphite powder, removing impurities, drying under argon protection, and standing; washing and drying grinding medium ceramic microspheres, and washing and drying grinding medium metal microspheres; and placing graphite powder, ceramic microspheres and metal microspheres at mass ratio of 1:1-5:1-5 in grinding cavity, vibrating and colliding metal microspheres by applying alternating electric field to drive ceramic microspheres and graphite to make disorder movement, and grinding for 0.5-1 hour. The metal microspheres are niobium, molybdenum, iron, nickel, tungsten, hafnium and zirconium microspheres. The size of metal microspheres is 0.01-0.1 mm. The size of ceramic microspheres is 0.1-1 mm.