• 专利标题:   Preparing supported high-entropy alloy material useful in hydrogen precipitation and oxygen reduction reaction, comprises e.g. dispersing carbon carrier in water, ultrasonically processing, adding metal salt aqueous solution and reducing agent aqueous solution, reacting, filtering, and drying.
  • 专利号:   CN115101764-A
  • 发明人:   YE W, GAO R, SONG Y
  • 专利权人:   UNIV DALIAN TECHNOLOGY
  • 国际专利分类:   B22F009/24, C22C030/00, C22C030/02, C22C030/06, C25B001/04, C25B011/065, C25B011/089, H01M004/88, H01M004/90, H01M004/92
  • 专利详细信息:   CN115101764-A 23 Sep 2022 H01M-004/92 202292 Chinese
  • 申请详细信息:   CN115101764-A CN10509301 10 May 2022
  • 优先权号:   CN10509301

▎ 摘  要

NOVELTY - Preparing supported high-entropy alloy material comprises dispersing the carbon carrier in water, ultrasonically processing for 0.5-1.5 hours, placing the mixture in a water bath, controlling the rotational speed to be more than 200 revolutions/minute at 0-25 °C, adding metal salt aqueous solution and reducing agent aqueous solution, reacting for 0.5-2 hours, suction filtering and washing the obtained mixed solution until the filtrate is neutral, drying to finally obtain a carbon-supported high-entropy alloy material, where the concentration of the carbon carrier dispersed in the aqueous solution is 0.1-2 mg/ml, the concentration of the metal salt aqueous solution is 0.1-30 mmol/l, the concentration of the reducing agent aqueous solution is 0.5-300 mmol/l, and the loading of the high-entropy alloy in the carbon-supported high-entropy alloy material is 5-60 wt.%. USE - The material is useful in hydrogen precipitation and oxygen reduction reaction (claimed). ADVANTAGE - The method is environmentally friendly and low-temperature and provides carbon supported high-entropy alloy material with high electro-catalytic activity, and has low energy consumption, and does not generate other difficult to process waste liquid and so on, belonging to green preparation route. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for supported high-entropy alloy material prepared by the above method.