• 专利标题:   Preparing silver-tin dioxide-reduced graphene oxide aerogel gas-sensitive material comprises (1) taking e.g. tin source, taking prepared silver-tin dioxide- reduced graphene oxide sol, placing container, aging solution and drying.
  • 专利号:   CN111122666-A
  • 发明人:   SHEN X, YAN W, CUI S, ZHU K, SONG Z
  • 专利权人:   UNIV NANJING TECHNOLOGY, UNIV NANJING TECHNOLOGY SUQIAN NEW MATER
  • 国际专利分类:   B22F009/24, B82Y030/00, B82Y040/00, C01G019/02, G01N027/12
  • 专利详细信息:   CN111122666-A 08 May 2020 G01N-027/12 202045 Pages: 11 Chinese
  • 申请详细信息:   CN111122666-A CN11387387 30 Dec 2019
  • 优先权号:   CN11387387

▎ 摘  要

NOVELTY - Preparing silver-tin dioxide-reduced graphene oxide aerogel gas-sensitive material comprises (1) taking tin source, silver source and reducing agent into deionized water, stirring for period of time, cross-link by adding alcohol solution and graphene oxide solution, adding alkaline reagent to adjust the pH value and sonicating, placing in hydrothermal reactor to react, (2) taking prepared silver-tin dioxide- reduced graphene oxide sol and placing container, allowing gel stand still and pouring aging solution and (3) adding the silver-tin dioxide-reduced graphene oxide sol obtained into a freeze dryer at -55 to -60 degrees C under the pressure is 1-5 Pa for 36-72 hours, taking out sample after temperature of freeze dryer reaches room temperature and (4) drying at elevated temperature silver-tin dioxide-reduced graphene oxide aerogel initially formed in step (3) is placed in vacuum drying box to continue drying to obtain an silver-tin dioxide-reduced graphene oxide aerogel material. USE - The method is useful for preparing silver-tin dioxide-reduced graphene oxide aerogel gas-sensitive material. ADVANTAGE - The method: can enhance reaction activity; reduces activation energy and negative effects caused by impurities; improves preparation efficiency, sample purity and material selectivity; is simple and easy.