• 专利标题:   Preparation of reduction-oxidation graphene composite zinc metasilicate quantum dot photocatalyst, involves dissolving reduced graphene oxide and zinc oxide in water, adding potassium stannate and urea, reacting, and filtering.
  • 专利号:   CN112473648-A
  • 发明人:   GAO P, WANG J
  • 专利权人:   UNIV HANGZHOU NORMAL
  • 国际专利分类:   B01J023/14, B01J035/00, B82Y030/00, C09K011/02, C09K011/66
  • 专利详细信息:   CN112473648-A 12 Mar 2021 B01J-023/14 202130 Pages: 11 Chinese
  • 申请详细信息:   CN112473648-A CN11210356 03 Nov 2020
  • 优先权号:   CN11210356

▎ 摘  要

NOVELTY - Preparation of reduction-oxidation graphene composite zinc metasilicate quantum dot photocatalyst, involves adding glucose to graphene oxide solution, stirring until glucose is completely dissolved, adding aqueous ammonia to solution (I), mixing to obtain solution (II), heating and reacting solution (II) in a water bath, cooling to room temperature, centrifuging and separating out the sample, washing with deionized water and absolute ethanol, drying to obtain reduced graphene oxide, adding the reduced graphene oxide and zinc oxide to distilled water, ultrasonically dissolving to obtain solution (III), adding potassium stannate and urea to solution (III), stirring to obtain solution (IV), reacting solution (IV) under heating and pressurizing conditions, cooling and filtering to obtain a white precipitate, washing the collected white precipitate, centrifuging and separating, and drying. USE - Preparation of reduction-oxidation graphene composite zinc metasilicate quantum dot photocatalyst. ADVANTAGE - The method provides quantum dots with an average particle diameter of 3-5 nm. Graphene has excellent electron transport property. The obtained photocatalyst has large specific surface area, broad light absorption region, improved separation rate of electrons and holes, and excellent photocatalytic efficiency in visible range.