• 专利标题:   Method for preparing bacterial cellulose graphene paper loaded nickel hydroxide electrode material as electrode material in supercapacitors, involves immersing cellulose in water, placing cellulose slurry into filtration, and heating.
  • 专利号:   CN105428091-A, CN105428091-B
  • 发明人:   HUANG Y, LIU L, LIU R, MA L, SUN S, WANG F, ZHAO F
  • 专利权人:   HARBIN INST TECHNOLOGY, HARBIN INST TECHNOLOGY
  • 国际专利分类:   H01G011/12, H01G011/30, H01G011/38, H01G011/86
  • 专利详细信息:   CN105428091-A 23 Mar 2016 H01G-011/86 201627 Pages: 8 English
  • 申请详细信息:   CN105428091-A CN10990854 25 Dec 2015
  • 优先权号:   CN10990854

▎ 摘  要

NOVELTY - A bacterial cellulose graphene paper loaded nickel hydroxide electrode material preparing method involves immersing bacterial cellulose in deionized water, ultrasonic washing, dispersing in water and transferring to a high-speed stirring to obtain bacterial cellulose pulp. The bacteria cellulose slurry is placed into filtration, acidified to continue suction graphene dispersion formed. Nickel and ammonium salts are dissolved in water, the bacterial cellulose graphite alkenyl paper is soaked in a nickel salt solution, aqueous ammonia is added, transferred to kettle, followed by heating. USE - Method for preparing bacterial cellulose graphene paper loaded nickel hydroxide electrode material that is utilized as flexible electrode material as anode material in supercapacitors (all claimed). ADVANTAGE - The material has high specific capacitance, high magnification, better mechanical properties of flexible electrode to prepare a super capacitor with better capacitance. DETAILED DESCRIPTION - A bacterial cellulose graphene paper loaded nickel hydroxide electrode material preparing method involves immersing bacterial cellulose in deionized water, ultrasonic washing, dispersing in deionized water and transferring to a high-speed stirring in a homogenizer, to obtain bacterial cellulose pulp. The acidified ultrasonic graphene is dispersed in deionized water to give graphene dispersion. The bacteria cellulose slurry is placed into pump vacuum filtration, acidified to continue suction graphene dispersion formed, and placed in a vacuum oven and dried to prepare a bacterial cellulose graphene paper. Nickel and ammonium salts are dissolved in distilled water, the bacterial cellulose graphite alkenyl paper is soaked in a nickel salt solution, aqueous ammonia is added, mixed evenly transferred to a reaction kettle, followed by heating to obtain product, where the bacterial cellulose bacterial cellulose paper graphene and acidified graphene mass ratio is (3-30): 1, and nickel salt with ammonium salt at molar ratio is (0.2~10): 1 and the ratio of a nickel salt with ammonia is 1 mmol: (0.5-5ml).