• 专利标题:   Preparing graphene, comprises e.g. taking aqueous solution of graphene oxide, cooling, adjusting pH of aqueous solution graphene oxide using a pH adjusting agent, and adjusting pH using pH reducing agent.
  • 专利号:   CN105399087-A, CN105399087-B
  • 发明人:   AN J, SONG M
  • 专利权人:   AN J, SONG M, SONG M
  • 国际专利分类:   C01B031/04, C01B032/184, C01B032/198
  • 专利详细信息:   CN105399087-A 16 Mar 2016 C01B-031/04 201632 Pages: 21 English
  • 申请详细信息:   CN105399087-A CN10920039 11 Dec 2015
  • 优先权号:   CN10920039

▎ 摘  要

NOVELTY - Preparing graphene, comprises (i) taking 0.2-1 g/l aqueous solution of graphene oxide, maintaining at 60-100 degrees C for at least 30 minutes, preferably 30-300 minutes, cooling to not greater than 20 degrees C, preferably 10-15 degrees C; (ii) adjusting pH of aqueous solution graphene oxide using a pH adjusting agent to 6-12; and (iii) adjusting pH of step (ii) product using pH reducing agent. USE - The method is useful for preparing graphene (claimed). ADVANTAGE - The method reduces the utilization amount of reduction agent, shortens the preparation time, and produces product with high purity.