• 专利标题:   High-mass transfer of chemical vapor deposition used for producing graphene, involves spin coating layer having polymethyl methacrylate on substrate, dispersing copper foil in corrosive liquid and processing loaded substrate with anisole.
  • 专利号:   CN102351175-A
  • 发明人:   LIU J, TANG Q, JI W, GUO X
  • 专利权人:   UNIV SOUTHEAST
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102351175-A 15 Feb 2012 C01B-031/04 201266 Pages: 5 Chinese
  • 申请详细信息:   CN102351175-A CN10342036 03 Nov 2011
  • 优先权号:   CN10342036

▎ 摘  要

NOVELTY - A layer with uniform thickness and containing polymethyl methacrylate is spin coated on a copper foil as substrate with thickness of 0.5-1 mm. The copper foil is dissolved using a dissolving agent comprising ammonium persulfate. The copper foil is dispersed in corrosive liquid, to obtain polymethyl methacrylate-coated graphite film. The polymethyl methacrylate-coated graphite film is attached on clean glass component, and cleaned. The loaded substrate is processed with anisole, and benzaldehyde is provided. The graphite substrate is cleaned and dried. USE - High-mass transfer of chemical vapor deposition used for producing graphene. ADVANTAGE - The method enables efficient and stable high-mass transfer of chemical vapor deposition of graphene. DETAILED DESCRIPTION - A layer with uniform thickness and containing polymethyl methacrylate is spin coated on a copper foil as substrate with thickness of 0.5-1 mm using colloid containing polymethyl methacrylate concentration of 0.1-0.13 mol/L. The size of copper foil is 6 cm2. The copper foil is dissolved using a dissolving agent comprising ammonium persulfate. The copper foil is dispersed in corrosive liquid, to obtain polymethyl methacrylate-coated graphite film. The polymethyl methacrylate-coated graphite film is attached on clean glass component, and ultrasonic cleaned using deionized water and residual water is dried at 90-100 degrees C. The loaded substrate is processed with anisole, and benzaldehyde is provided. The graphite substrate is cleaned and dried.