• 专利标题:   Preparing flame retardant non-woven fabric comprises e.g. adding prepared flame retardant electro-spinning liquid into upper glue groove, rolling and unrolling, horizontal and uniform rewinding, depositing on the upper non-woven fabric on upper non-woven fabric, cleaning and drying.
  • 专利号:   CN114108185-A
  • 发明人:   LIN L, WU X, WANG J, CHEN C, CUI D
  • 专利权人:   SHANGHAI NAT ENG RES CENT NANOTECHNOLOGY
  • 国际专利分类:   D01F001/07, D01F006/50, D04H001/4309, D04H001/728
  • 专利详细信息:   CN114108185-A 01 Mar 2022 D04H-001/728 202236 Chinese
  • 申请详细信息:   CN114108185-A CN11465856 03 Dec 2021
  • 优先权号:   CN11465856

▎ 摘  要

NOVELTY - Preparing flame retardant non-woven fabric comprises e.g. (i) taking 5-10 pts. wt. graphene, 1-2 pts. wt. isocyanate propyl triethoxy silane, 0.1-0.2 pts. wt. n-butyltin dilaurate and 900-1800 pts. wt. tetrahydrofuran, pouring according to sequence into wet grinding device, using grinding medium as zirconium oxide microsphere, pre-mixing, pouring into wet grinding device, grinding at 2000 revolution/minute at below 3degrees Celsius for 2 hours, discharging, adding 12-24 pts. wt. hydrochloric acid and 100-200 pts. wt. de-ionized water, refluxing and stirring for 12 hours under the protection of nitrogen at 60degrees Celsius to obtain the graphene solution, taking 50 pts. wt. phosphorus-containing silicone 9,10-Dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO)-(vinyltrimethoxysilane) VTS, dissolving in 450 pts. wt. tetrahydrofuran, adding into graphene solution, adding 10 pts. wt. aqueous ammonia and stirring for 5 hours to obtain the flame retardant solution containing graphene. USE - The method is useful for preparing flame retardant non-woven fabric. ADVANTAGE - The method: can spray compounded fuel-resistant slurry to the non-woven fabric covered on the metal substrate by a strong electric field force to form filaments; controls the moving speed of the non-woven fabric in the horizontal direction; and covers the non-woven fabric substrate with a comprehensive and uniform flame retardant fiber thus after cleaning and drying and obtains a flame retardant non-woven fabric sample with good flame retardant index. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for flame retardant non-woven fabric, prepared as mentioned above.