• 专利标题:   Preparation of fluorinated graphene involves fluorinating graphene with fluorinating agent to obtain graphene crude and fluorinating crude graphene with another fluorinating agent, under inert gas protection.
  • 专利号:   CN105883745-A, WO2017174043-A2, WO2017174043-A3, CN105883745-B, US2019100436-A1
  • 发明人:   YAN J
  • 专利权人:   YAN J, ZHANG L, YAN J, ZHANG L
  • 国际专利分类:   C01B031/00, C01B032/182, C01B032/194
  • 专利详细信息:   CN105883745-A 24 Aug 2016 C01B-031/00 201674 Pages: 12 Chinese
  • 申请详细信息:   CN105883745-A CN10214775 07 Apr 2016
  • 优先权号:   CN10214775

▎ 摘  要

NOVELTY - Preparation of fluorinated graphene involves (a) fluorinating graphene with fluorinating agent (1) under the protection of inert gas at 150-550 degrees C for 2-20 hours to obtain the crude product of graphene and (b) fluorinating crude graphene with fluorinating agent (2) under the protection of inert gas at 150-400 degrees C for 2-10 hours to obtain fluorinated graphene. The graphene is chosen from graphene powder and graphene film. The fluorinating agent (1) is fluorine gas. The fluorinating agent (2) is gas phase fluoride. USE - Preparation of fluorinated graphene (claimed). ADVANTAGE - The method prepares high fluorine content of fluorinated graphene with low density defect, and fluorine content is close to the theoretical value level.