• 专利标题:   Manufacture of graphene film material involves growing graphene film on copper substrate, providing on silicon substrate, dissolving copper substrate in ferric nitrate solution, depositing graphene film, drying, cleaning and cooling.
  • 专利号:   CN102020263-A, CN102020263-B
  • 发明人:   ZHANG X, JIANG J, YU W, ZHANG L
  • 专利权人:   UNIV ZHEJIANG
  • 国际专利分类:   C01B031/02, C23C016/26
  • 专利详细信息:   CN102020263-A 20 Apr 2011 C01B-031/02 201152 Pages: 8 Chinese
  • 申请详细信息:   CN102020263-A CN10218410 02 Jul 2010
  • 优先权号:   CN10218410

▎ 摘  要

NOVELTY - A graphene film is grown on a copper substrate using mixed atmosphere of hydrogen and methane by chemical vapor deposition method. The copper substrate with graphene film is provided on silicon substrate, silicon substrate is provided into ferric nitrate solution, copper substrate is dissolved, and graphene film is deposited on silicon substrate. The solution is diluted, silicon substrate deposited with graphene is taken from the solution, and dried. The silicon substrate is cleaned, placed into annealing furnace protected by argon gas, cooled, and graphene film material is manufactured. USE - Manufacture of graphene film material. ADVANTAGE - The graphene film material is easily and efficiently manufactured with high quality. DETAILED DESCRIPTION - A graphene film is grown on a copper substrate using mixed atmosphere of hydrogen and methane by chemical vapor deposition method. The copper substrate with graphene film is provided on silicon substrate with oxidized surface, the silicon substrate is provided into ferric nitrate solution, copper substrate is dissolved, and graphene film is deposited on the silicon substrate. The solution is diluted, the silicon substrate deposited with graphene is taken from the solution, and dried with vacuum drying tank. The silicon substrate deposited with graphene is ultrasonically cleaned, placed into annealing furnace protected by argon gas, cooled into room temperature with furnace, and graphene film material is manufactured.