• 专利标题:   Manufacture of cobalt ferrite/graphene magnetic nano composite powder involves mixing graphite oxide solution and metal salt solution, adding reaction liquid into reaction kettle, cooling, washing and drying.
  • 专利号:   CN102276244-A
  • 发明人:   CHEN X, HOU C, LI Y, WANG H, ZHANG Q
  • 专利权人:   UNIV DONGHUA
  • 国际专利分类:   C04B035/26, C04B035/28, C04B035/32, C04B035/626
  • 专利详细信息:   CN102276244-A 14 Dec 2011 C04B-035/26 201232 Pages: 8 Chinese
  • 申请详细信息:   CN102276244-A CN10134824 19 May 2011
  • 优先权号:   CN10134824

▎ 摘  要

NOVELTY - Graphite oxide and a metal salt are dispersed in glycol solution after dissolving metal salt solution in polyethylene glycol and anhydrous sodium acetate. Graphite oxide solution and metal salt solution are mixed. The metal salt is cobalt salt, nickel salt, or iron salt. The reaction liquid is added into a reaction kettle, the temperature is raised to 180-220 degrees C, reacted for 8-16 hours, cooled to room temperature, collected by magnet, washed using deionized water and absolute ethyl alcohol, and dried. USE - Manufacture of cobalt ferrite/graphene magnetic nano composite powder. ADVANTAGE - The cobalt ferrite/graphene magnetic nano composite powder is easily manufactured with favorable dispersibility and high magnetization intensity. DETAILED DESCRIPTION - Graphite oxide and a metal salt in mass ratio of 1:1-1:10 are dispersed in glycol solution after dissolving metal salt solution in polyethylene glycol and anhydrous sodium acetate. Graphite oxide solution and metal salt solution are mixed. The metal salt is cobalt salt, nickel salt, or iron salt. The molar ratio of cobalt ion and nickel ion is 4:1-1:4. The molar ratio of cobalt ion and nickel, with respect to iron ion is 1:2. The reaction liquid is added into a reaction kettle, the temperature is raised to 180-220 degrees C, reacted for 8-16 hours, cooled to room temperature, collected by magnet, washed using deionized water and absolute ethyl alcohol, and dried.