• 专利标题:   Preparing modified graphene used for preparing thermally conductive polybutylene terephthalate material, involves adding graphene to hydrochloric acid, performing ultrasonic filtration, and adding concentrated hydrochloric acid.
  • 专利号:   CN113831595-A
  • 发明人:   JIANG C, ZOU C, YAO C, WU A, YANG G
  • 专利权人:   HEFEI GENIUS ADVANCED MATERIAL CO LTD
  • 国际专利分类:   C08K003/04, C08K005/098, C08K005/20, C08K009/02, C08L067/02, C09K005/14
  • 专利详细信息:   CN113831595-A 24 Dec 2021 C08K-009/02 202255 Chinese
  • 申请详细信息:   CN113831595-A CN10588945 24 Jun 2020
  • 优先权号:   CN10588945

▎ 摘  要

NOVELTY - Preparing modified graphene involves adding 1 pts. wt. graphene to 28-30 wt.% hydrochloric acid for 3-5 minutes, performing ultrasonic filtration, adding to 15-18 wt.% concentrated hydrochloric acid, standing for 6-8 hours, washing after separation, and drying to obtain a modified graphene. USE - Method for preparing modified graphene used for preparing thermally conductive polybutylene terephthalate material (claimed). ADVANTAGE - The prepared polybutylene terephthalate has excellent thermal conductivity. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1)a thermally conductive polybutylene terephthalate material, which comprises: 100 pts. wt. polybutylene terephthalate, 1-3 pts. wt. modified graphene, 0.5-1 pts. wt. lubricant and 0.5-1 pts. wt. antioxidant are preparing with specific weight portion, where modified graphene is prepared by adding 1 pts. wt. graphene to 28-30 wt.% hydrochloric acid for 3-5 minutes, performing ultrasonic filtration, adding to 15-18% concentrated hydrochloric acid, standing for 6-8 hours, washing after separation, and drying to obtain a modified graphene; and (2)a method for preparing thermally conductive polybutylene terephthalate material, which involves: (a)mixing fully polybutylene terephthalate, modified graphene, lubricant and antioxidant with specific ratio to obtain uniform mixture;(b)adding mixed material into a twin-screw extruder;(c)melting;(d)extruding;(e)pelletizing;(d)drying to obtain the thermally conductive polybutylene terephthalate material.