• 专利标题:   Palladium nanodendrite-graphene nanocomposite-based hydrogen sensor obtained by mixing palladium nanodendrite synthesized by reduction ratio of palladium precursor salt in graphene and cetrimonium bromide using palladium nanodendrite.
  • 专利号:   WO2016017858-A1, KR2016014925-A, KR1613437-B1
  • 发明人:   CHUNG G, CHUNG G S
  • 专利权人:   UNIV ULSAN FOUND IND COOP
  • 国际专利分类:   B82B003/00, G01N027/12
  • 专利详细信息:   WO2016017858-A1 04 Feb 2016 G01N-027/12 201614 Pages: 25
  • 申请详细信息:   WO2016017858-A1 WOKR010104 27 Oct 2014
  • 优先权号:   KR097097

▎ 摘  要

NOVELTY - Palladium nanodendrite-graphene nanocomposite-based hydrogen sensor obtained by mixing palladium nanodendrite which is synthesized by the reduction ratio of the palladium precursor salt in graphene and cetrimonium bromide environment by using palladium nanodendrite as catalyst for detecting hydrogen, is claimed. USE - Used as palladium nanodendrite-graphene nanocomposite-based hydrogen sensor. ADVANTAGE - The sensor has good repeatability even at room temperature and high reaction value of 25%, detects hydrogen of various concentrations with good linearity over a wide range, and exhibits quick response/recovery time. DETAILED DESCRIPTION - Palladium nanodendrite-graphene nanocomposite-based hydrogen sensor obtained by either: mixing palladium nanodendrite which is synthesized by the reduction ratio of the palladium precursor salt in graphene and cetrimonium bromide environment by using palladium nanodendrite as catalyst for detecting hydrogen; or (a) adding ascorbic acid solution and potassium tetrachloropalladate(II) into deionized water, stirring, and preparing mixture solution by aiding cetyltrimethylammonium bromide while stirring, (b) centrifuging the obtained mixture solution, spreading multiple times from the deionized water to remove the reaction product, and synthesizing palladium nanodendrite solution by re-spreading palladium suspension solution from the deionized water, (c) adding palladium nanodendrite solution into graphene oxide aqueous solution containing pure graphite powder, stirring, and forming mixture of palladium nanodendrite-graphene hybrid by adding reducing agent while stirring at a temperature higher than room temperature, (d) coating by spraying the mixture suspension solution of palladium nanodendrite-graphene hybrid on silicon dioxide/silicon base, and (e) forming an ohmic contacting layer by plating precious metals on the surface of the palladium dendrite-graphene/silicon dioxide/silicon base, is claimed.