• 专利标题:   Preparation of copper-based composite used e.g. for absorbing organic anionic dye, involves dissolving graphene oxide in deionized water, processing, dissolving copper source compound in graphene solution and dissolving sodium hydroxide.
  • 专利号:   CN113908802-A
  • 发明人:   LI W, LIU S
  • 专利权人:   UNIV TIANJIN TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/30, C02F001/28, C02F101/30
  • 专利详细信息:   CN113908802-A 11 Jan 2022 B01J-020/20 202232 Chinese
  • 申请详细信息:   CN113908802-A CN11110591 23 Sep 2021
  • 优先权号:   CN11110591

▎ 摘  要

NOVELTY - A copper-based composite is prepared by dissolving graphene oxide in deionized water, ultrasonically processing to completely disperse, taking copper source compound as copper source, dissolving in graphene solution, dissolving 8-12 mol/L sodium hydroxide, orderly dropping little ethylenediamine solution and micro hydrazine hydrate (80%) solution to obtain graphene sheet with different length-diameter ratio of copper nanorod, reacting in water bath or oil bath at holding temperature of 50-90degrees Celsius, reacting for 0.5-4 hours, putting in tubular furnace, and reacting to 100-200degrees Celsius for 1-4 hours at rate of 3-10degrees Celsius/minute to obtain copper-copper(II) oxide-graphene oxide, copper oxide-copper(I) oxide-graphene oxide and copper-copper(I) oxide-graphene oxidenano rod. USE - The method is used for preparing copper-based composite used for absorbing organic anionic dye and in water purification field (all claimed). ADVANTAGE - The product has excellent adsorption effect.