• 专利标题:   Preparing graphene oxide with controllable pH, by placing graphene oxide slurry in ice-water bath, adding diluent and pH regulator to obtain mixed slurry, dispersing in ice-water bath, placing in vacuum oven and removing bubbles in slurry.
  • 专利号:   CN110482538-A
  • 发明人:   DUAN Y, ZHANG Y, ZHAO Z
  • 专利权人:   SHANGHAI LEVSON NANOTECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN110482538-A 22 Nov 2019 C01B-032/198 201998 Pages: 8 Chinese
  • 申请详细信息:   CN110482538-A CN10790398 26 Aug 2019
  • 优先权号:   CN10790398

▎ 摘  要

NOVELTY - Method for preparing graphene oxide with controllable pH, involves (i) placing the graphene oxide slurry in an ice-water bath for pretreatment, adding a diluent and stirring, (ii) adding the pH regulator in dropwise to the diluted graphene oxide slurry in step (i) to obtain a mixed slurry, where the pH regulator is an organic base, (iii) dispersing the mixed slurry obtained in step (ii) in the ice-water bath and stirring, and (iv) placing the mixed slurry obtained in step (iii) in a vacuum oven and keeping at room temperature until the bubbles in the slurry are completely removed. USE - Method for preparing graphene oxide with controllable pH. ADVANTAGE - The method stably controls and adjusts the pH of graphene oxide without affecting the performance of graphene.