• 专利标题:   Preparing conductive composite material for ion batteries by adding graphene to solvent of dispersant, mixing uniformly, adding vinylidene fluoride monomer, initiator and pH adjuster to graphene dispersion under inert gas atmosphere condition, polymerizing, centrifuging and drying polymer product.
  • 专利号:   CN114085339-A, CN114085339-B
  • 发明人:   SUN D, ZHUANG C, WANG Y, LIN J, HUANG W, FANG C, LIN L, HUANG C, HONG J
  • 专利权人:   XIAMEN KNANO GRAPHENE TECHNOLOGY CO LTD
  • 国际专利分类:   C08F214/22, C08F292/00, C08K003/04, C08K007/06, C08L051/10, H01B001/12, H01B013/00, H01M004/62
  • 专利详细信息:   CN114085339-A 25 Feb 2022 C08F-292/00 202235 Chinese
  • 申请详细信息:   CN114085339-A CN11451171 30 Nov 2021
  • 优先权号:   CN11451171

▎ 摘  要

NOVELTY - Method for preparing a conductive composite material for ion batteries, involves (a) adding 1-20 pts. wt. graphene to a solvent of 100-1000 pts. wt. dispersant, and mixing uniformly to obtain a graphene dispersion, (b) under the condition of inert gas atmosphere and preset pressure, adding 20-100 pts. wt. vinylidene fluoride monomer, 0.2-1 pt. wt. initiator and 0.01-1 pt. wt. pH adjuster to 20-100 pts. wt. graphene dispersion, mixing uniformly, and polymerizing at low temperature for a certain period of time to obtain a polymer product, and (c) centrifuging and drying the polymer product to obtain a polyvinylidene fluoride/graphene conductive composite material. USE - The method is used for preparing a conductive composite material which is used in a conductive paste for ion batteries (all claimed). ADVANTAGE - The method effectively improves the mechanical properties and electrical properties of the conductive composite material and the conductive paste, and optimizes the electrical properties of the ion battery. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) a method for preparing a conductive paste for ion batteries, comprising (i) adding 1-10 pts. wt. polyvinylidene fluoride/graphene conductive composite material and 0.5-10 pts. wt. conductive carbon material to 80-98.5 pts. wt. organic solvent, and mixing uniformly to obtain a premix, (ii) grinding the premix obtained in step (i), and after grinding for 3-5 hours, obtaining a polyvinylidene fluoride/graphene conductive slurry; and (2) a conductive paste for ion batteries comprising 1-10 pts. wt. polyvinylidene fluoride/graphene conductive composite material, 0.5-10 pts. wt. conductive carbon material and 80-98.5 pts. wt. organic solvent.