• 专利标题:   Graphene-polyimide resin thermally conductive composite material for producing carbon composite material, is obtained by dispersing expanded graphite in N-methylpyrrolidone, reacting, immersing in polyimide solution, depositing and stacking.
  • 专利号:   CN110776737-A
  • 发明人:   FENG Y, GAO L, FENG W, ZHANG F, LV F
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   C08K003/04, C08L079/08, C09K005/14
  • 专利详细信息:   CN110776737-A 11 Feb 2020 C08L-079/08 202022 Pages: 8 Chinese
  • 申请详细信息:   CN110776737-A CN10858290 31 Jul 2018
  • 优先权号:   CN10858290

▎ 摘  要

NOVELTY - A graphene-polyimide resin thermally conductive composite material has a thermal conductivity of 14-20 W/(m.K) along the material axis, and is obtained by (i) dispersing 0.1-0.5 part mass expanded graphite in 100-150 parts mass N-methylpyrrolidone and reacting at 140-160 degrees C for 5-10 hours, centrifuging obtained dispersion by ultrasound, removing the supernatant, suction filtering using N-methyl-2-pyrrolidone, washing with water and ultrasonically processing, and freeze-drying to obtain graphene powder, (ii) placing obtained graphene powder in a plasma-enhanced chemical vapor deposition system device, vacuuming, heating to 500-700 degrees C, passing a carbon source gas, turning on the plasma source for vertical growth of graphene, cooling to room temperature of 20-25 degrees C to obtain a sample of vertical graphene grown on the graphene surface and passing inert protective gas, and (iii) immersing the obtained sample in a polyimide solution, depositing and stacking by suction filtration. USE - Graphene-polyimide resin thermally conductive composite material is used for producing carbon composite material. ADVANTAGE - The graphene-polyimide resin thermally conductive composite material has improved thermal conductivity and mechanical properties. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of graphene-polyimide resin thermally conductive composite material.