• 专利标题:   Preparation of graphene-carbon nanotube thin film for electrochemical capacitor involves dispersing graphite oxide in deionized water, dispersing carbon nanotube in ethanol, mixing dispersions, removing solvents, heating, and cooling.
  • 专利号:   CN103787311-A
  • 发明人:   LIU D, WANG Y, ZHONG H, ZHOU M
  • 专利权人:   OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING ENG CO LTD, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/02, C01B031/04, H01G011/84
  • 专利详细信息:   CN103787311-A 14 May 2014 C01B-031/04 201446 Pages: 11 Chinese
  • 申请详细信息:   CN103787311-A CN10428433 31 Oct 2012
  • 优先权号:   CN10428433

▎ 摘  要

NOVELTY - Graphene-carbon nanotube thin film is prepared by oxidizing graphite to obtain graphite oxide, ultrasonically dispersing in deionized water for 1-2 hours to obtain 0.5-1 g/L graphite oxide dispersion (S102), ultrasonically dispersing carbon nanotube for 3-6 hours to obtain 0.2-1 g/L carbon nanotube dispersion (S103), ultrasonically mixing graphite oxide and carbon nanotube dispersion to obtain liquid mixture, removing deionized water and ethanol to obtain graphite oxide-carbon nanotube thin film (S104), heating, and cooling to room temperature (S105). USE - Preparation of graphene-carbon nanotube thin film for electrochemical capacitor (claimed). ADVANTAGE - The preparation of graphene-carbon nanotube thin film prevents agglomeration of graphene sheet, improves surface energy storage, and increases electrochemical capacity of electrode capacitor. DETAILED DESCRIPTION - Graphene-carbon nanotube thin film is prepared by oxidizing graphite to obtain graphite oxide, ultrasonically dispersing in deionized water for 1-2 hours to obtain 0.5-1 g/L graphite oxide dispersion, ultrasonically dispersing carbon nanotube for 3-6 hours to obtain 0.2-1 g/L carbon nanotube dispersion, ultrasonically mixing graphite oxide and carbon nanotube dispersion with volume ratio of 1:1-1:2 for 5-8 hours to obtain liquid mixture, removing deionized water and ethanol to obtain graphite oxide-carbon nanotube thin film, heating under inert gas atmosphere at 700-900 degrees C for 0.5-2 hours, and cooling to room temperature. An INDEPENDENT CLAIM is included for application of graphene-carbon nanotube thin film for electrochemical capacitor which involves rolling graphene-carbon nanotube thin film, drying, slicing to obtain electrode plate, and stacking to obtain electric core which is coated with outer shell containing inner electrolyte. DESCRIPTION OF DRAWING(S) - The drawing shows a flow chart for preparation of graphene-carbon nanotube thin film. (Drawing includes non-English language text). Preparation of graphite oxide (S101) Preparation of graphite oxide dispersion (S102) Preparation of carbon nanotube dispersion (S103) Preparation of graphite oxide-carbon nanotube thin film (S104) Preparation of graphene-carbon nanotube thin film (S105)