• 专利标题:   Producing carbon fiber composite material involves dispersing graphene oxide in solvent to obtain graphene oxide suspension, and then adding diamine and catalyst with stirring.
  • 专利号:   CN105233794-A, CN105233794-B
  • 发明人:   CHEN F, JIN G, SU J
  • 专利权人:   UNIV HEFEI TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/30, C02F001/28, C02F101/20, G21F009/12
  • 专利详细信息:   CN105233794-A 13 Jan 2016 B01J-020/20 201634 Pages: 12 English
  • 申请详细信息:   CN105233794-A CN10703334 26 Oct 2015
  • 优先权号:   CN10703334

▎ 摘  要

NOVELTY - Carbon fiber composite material preparation involves dispersing graphene oxide in a solvent to obtain graphene oxide suspension, adding diamine and catalyst at 20-120 degrees C with stirring for 1-5 hours, filtering the resulting mixture, and then drying to give amine thin graphite. Polyacrylonitrile conductive carbon fibers as working electrode are immersed in 9.8 g/l sulfuric acid solution to generate carboxyl carbon fibers. The generated carboxyl carbon fibers are immersed in suspension at 20-120 degrees C with stirring for 1-5 hours to produce graphene modified carbon fibers. USE - Method for producing carbon fiber composite material (claimed). ADVANTAGE - The method produces the carbon fiber composite material in a simple manner with excellent selective adsorption capacity. DETAILED DESCRIPTION - Carbon fiber composite material preparation involves dispersing graphene oxide in a solvent to obtain graphene oxide suspension, adding diamine and catalyst at 20-120 degrees C with stirring for 1-5 hours, filtering the resulting mixture, and then drying to give amine thin graphite. Polyacrylonitrile conductive carbon fibers as working electrode are immersed in 9.8 g/l sulfuric acid solution to generate carboxyl carbon fibers. The generated carboxyl carbon fibers are immersed in suspension at 20-120 degrees C with stirring for 1-5 hours to produce graphene modified carbon fibers. The produced graphene modified carbon fibers are immersed in suspension with catalyst at 20-120 degrees C with stirring for 1-5 hours to produce graphene bilayer modified carbon fibers. The resulting produce graphene bilayer modified carbon fibers, the carboxyl carbon fibers and the aphene modified carbon fibers are mixed to generate a multi-layered carbon fiber composite carrier. Potassium ferrocyanide solution is added in the generated multi-layered carbon fiber composite carrier to adjust pH to 2-7, and then immersed in potassium ferrocyanide solution for 10-50 minutes at 20-110 degrees C. The soaking process is repeated for 3-7 times to give the final carbon fiber composite material. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic scanning electron microscopic image of the carbon fiber composite material.