• 专利标题:   Preparing tellurene/graphene hybrid porous fiber having radial openings, comprises e.g. adding graphene oxide to tellurene pre-stripping dispersion liquid, centrifuging, washing, concentrating, drying and peforming wet spinning.
  • 专利号:   CN111636119-A
  • 发明人:   ZHANG H, MENG S
  • 专利权人:   UNIV SHENZHEN
  • 国际专利分类:   D01D001/02, D01D005/06, D01F009/08, H01L051/46
  • 专利详细信息:   CN111636119-A 08 Sep 2020 D01F-009/08 202081 Pages: 11 Chinese
  • 申请详细信息:   CN111636119-A CN10432612 20 May 2020
  • 优先权号:   CN10432612

▎ 摘  要

NOVELTY - Preparing tellurene/graphene hybrid porous fiber having radial openings, comprises adding graphene oxide to tellurene pre-stripping dispersion liquid and performing ultrasound in a constant temperature water bath, centrifuging, collecting the bottom layer mixture, dispersing the bottom layer mixture in water, washing, concentrating, drying to obtain mixture of tellurene and graphene oxide; adding water to mixture of tellurene and graphene oxide and stirring the mixture to obtain mixture, sonicating the mixture by pulsed tip ultrasound, concentrating the mixed solution to obtain tellurene/graphene oxide mixed dispersion; peforming wet spinning using tellurene/graphene oxide mixed dispersion as spinning dope, glacial acetic acid as coagulation bath, and stepped spinning needle with a larger inner diameter to obtain wet tellurene/graphene oxide hybrid fiber; and washing the wet tellurene/graphene oxide hybrid fiber until the fiber is neutral, drying and reducing to obtain final product. USE - The tellurene/graphene hybrid porous fiber having radial openings is useful in flexible photodetectors, battery electrodes and photocatalysis (claimed). ADVANTAGE - The method: solves the defects of tellurene easy to stack with each other, poor dispersibility in water and lack of spinnability.