• 专利标题:   Solid super acid catalyst used for preparing p-methoxy cinnamic acid isooctyl ester, comprises chromium oxide-silica as composite carrier, graphene as hard template, sulfuric acid as sulfur source, and modified solid super strong acid.
  • 专利号:   CN114029072-A
  • 发明人:   ZHANG Y, ZHANG D, JIANG P, GUO Y, LIU L
  • 专利权人:   WANHUA CHEM GROUP CO LTD
  • 国际专利分类:   B01J027/053, C07C067/08, C07C069/734
  • 专利详细信息:   CN114029072-A 11 Feb 2022 B01J-027/053 202223 Chinese
  • 申请详细信息:   CN114029072-A CN11452512 01 Dec 2021
  • 优先权号:   CN11452512

▎ 摘  要

NOVELTY - Solid super acid catalyst comprises Cr2O3-SiO2 as a composite carrier, graphene as a hard template, sulfuric acid as a sulfur source, X-SO42-/Cr2O3-SiO2 solid super strong acid modified by transition metal X. USE - Solid super acid catalyst used for preparing p-methoxy cinnamic acid isooctyl ester (claimed). ADVANTAGE - The solid acid catalyst helps to reduce the reaction temperature, also improves the conversion rate and the selectivity of the p-methoxy cinnamic acid, after the transition metal modification, and greatly improves the reaction strength and service life of catalyst. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing p-methoxy cinnamic acid isooctyl ester, which involves: taking p-methoxycinnamic acid and isooctanol as raw materials, alkane compound as solvent under the action of the X-SO42-/Cr2O3-SiO2 solid super acid catalyst.