• 专利标题:   Preparing hydroxylated graphene-polymer composite material, involves preparing hydroxylated graphene suspension by dissolving hydroxylated graphene in solvent, heating, ultrasonically processing, and adding polymer to dispersion.
  • 专利号:   CN104371226-A, CN104371226-B
  • 发明人:   DAI S, GENG X, YANG C, ZHANG X, YAN S
  • 专利权人:   AVIATION IND CORP CHINA BEIJING GREAT WA, AVIC BEIJING INST AERONAUTICAL MATERIALS
  • 国际专利分类:   C08K003/04, C08K009/00, C08L025/06, C08L027/12
  • 专利详细信息:   CN104371226-A 25 Feb 2015 C08L-027/12 201532 Pages: 7 Chinese
  • 申请详细信息:   CN104371226-A CN10638440 06 Nov 2014
  • 优先权号:   CN10638440

▎ 摘  要

NOVELTY - The method involves preparing hydroxylated graphene suspension by dissolving hydroxylated graphene in solvent, heating, ultrasonically processing to disperse uniformly, adding polymer to obtain hydroxylated graphene-polymer turbid solution, heating to obtain homogeneous hydroxylated graphene-polymer turbid solution, cooling obtained product, adding volatile solvent to hydroxylated graphene-polymer turbid solution, filtering under vacuum conditions and then drying to obtain hydroxylated graphene-polymer powder, and drying obtained powder in oven to obtain composite. USE - The method is useful for preparing hydroxylated graphene-polymer composite material (claimed). ADVANTAGE - The method is capable of preparing hydroxylated graphene-polymer composite material with controlled dielectric constant and improved electrical properties. DETAILED DESCRIPTION - The method involves preparing hydroxylated graphene suspension by dissolving hydroxylated graphene in organic solvent including N,N-dimethylformamide or tetrahydrofuran, heating the suspension having a concentration of 0.1-0.30 mg/ml, ultrasonicating the suspension for 30-60 minutes to disperse uniformly, adding polymer including polystyrene or polyvinylidene fluoride to the dispersion at a mass ratio of 0.1-30:1000 to obtain a hydroxylated graphene-polymer turbid solution, heating the solution at 70-90 degrees C for 0.5-1 hour to obtain a homogeneous hydroxylated graphene-polymer turbid solution, cooling the obtained product, adding a volatile solvent including ethanol or acetone to the hydroxylated graphene-polymer turbid solution at a volume ratio of 1:2, filtering under vacuum conditions and then drying to obtain hydroxylated graphene-polymer powder, and drying the obtained powder at 40-60 degrees C for 24-48 hours in an oven to obtain a composite.