• 专利标题:   Resource utilization method of phosphoric acid-contains waste sulfuric acid liquid used for preparing graphene oxide, involves detecting phosphate content, sulfate content in phosphate, adding acidic solution, and stirring fully.
  • 专利号:   CN114195178-A, CN114195178-B
  • 发明人:   LI P, GONG W, CAO A, WANG W, HOU S, SONG X, LIU T
  • 专利权人:   SHANDONG JINLITE NEW MATERIAL CO LTD
  • 国际专利分类:   C01B025/32, C01D003/04, C01D003/14, C01F011/46
  • 专利详细信息:   CN114195178-A 18 Mar 2022 C01F-011/46 202238 Chinese
  • 申请详细信息:   CN114195178-A CN10051325 17 Jan 2022
  • 优先权号:   CN10051325

▎ 摘  要

NOVELTY - Resource utilization method of phosphoric acid-contains waste sulfuric acid liquid involves preparing waste sulfuric acid solution contains phosphorus acid in target object, detecting phosphate content and sulfate content in phosphate, taking barium carbonate with amount of phosphate substance in target substance, adding acidic solution, fully stirring to prepare barium-carbonate slurry number one, taking phosphate substance of target material, adding acidic solution and fully stirring, slowly adding barium sulfate solution to target object to react, controlling pH of system at 6.5-7.5, separating solid and liquid to obtain primary filtrate, drying solid to obtain phosphate material, and performing reverse osmosis (RO) treatment on secondary filtrates to obtain chloride salt. USE - Resource utilization method of phosphoric acid-contains waste sulfuric acid liquid used in graphene industry fast development process for preparing graphene oxide. ADVANTAGE - The method enables to ensure processing of single ion and is not affected subsequent separation of other ions, and avoids presence of phosphoric acid separating effect of other ion, not only after processing single ion, also waste water reaches discharge standard; effectively finishes recovery of each ion according to specific order.