• 专利标题:   Method for preparing current collector graphene, involves using three-dimensional printing to print graphene oxide ink into fork pattern on substrate and drying, reducing dried fork pattern in reducing agent, and performing washing and drying process to obtain graphene current collector.
  • 专利号:   CN115939409-A
  • 发明人:   WANG G, WANG Y, SHI X, ZHANG Y, LI L
  • 专利权人:   UNIV XIAN JIAOTONG
  • 国际专利分类:   H01M010/38, H01M004/04, H01M004/66, H01M004/70
  • 专利详细信息:   CN115939409-A 07 Apr 2023 H01M-004/66 202339 Chinese
  • 申请详细信息:   CN115939409-A CN11691248 27 Dec 2022
  • 优先权号:   CN11691248

▎ 摘  要

NOVELTY - The method involves using three-dimensional (3D) printing to print a graphene oxide ink into a fork pattern on a substrate and drying. The substrate is a silicon sheet, a glass sheet, a nylon sheet or a polyimide film. The dried fork pattern is reduced in reducing agent. A washing and drying process are performed to obtain a graphene current collector. The reducing agent is mixed solution of hydrogen iodide (HI) and acetic acid (CH3COOH). The graphene oxide ink is prepared by adding graphene oxide into a solvent and performing ball milling to obtain graphene oxide ink. The solvent is water and/or ethanol. USE - Method for preparing current collector graphene. ADVANTAGE - The method is simple and efficient, utilizes reduction graphene as the current collector to greatly reduce the manufacturing cost of zinc ion micro-battery and the preparation process without adding adhesive agent, and has good electrical conductivity without high-temperature post-treatment, which will not destroy the crystal structure of the electrode material, thus improving the electrochemical energy storage performance of the device. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for a method for preparing zinc ion micro-battery. DESCRIPTION OF DRAWING(S) - The drawing shows a scanning electron micrograph of the cathode material of the zinc ion micro-battery.