• 专利标题:   Synthesizing graphene/carbon-coated lithium iron phosphate small-scale nanocomposites through aniline polymerization confined effect involves dispersing graphite oxide and ferric iron salt in deionized water, and adding ammonium persulfate.
  • 专利号:   CN110444740-A
  • 发明人:   WANG D, WANG B, LI X, YUAN Y, CHEN Z, CHEN X, QIN X, MA N
  • 专利权人:   HARBIN INST TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/583, H01M004/62
  • 专利详细信息:   CN110444740-A 12 Nov 2019 H01M-004/36 201993 Pages: 10 Chinese
  • 申请详细信息:   CN110444740-A CN10411061 02 May 2018
  • 优先权号:   CN10411061

▎ 摘  要

NOVELTY - Synthesizing graphene/carbon-coated lithium iron phosphate small-scale nanocomposites through aniline polymerization confined effect involves dispersing graphite oxide and ferric iron salt in deionized water, and adding ammonium persulfate and mixing to obtain first solution, dissolving phosphate in deionized water at room temperature, adding aniline, and mixing to obtain second solution, mixing first solution and second solution at room temperature and continuously stirring for 4-12 hours to obtain the precursor material. The prepared precursor material is mixed with the lithium source in solid phase, and then an organic small molecular carbon source is added, and ground uniformly in a protective atmosphere furnace with inert gas and/or a reducing gas, continuously increase the temperature to 550-750 degrees C at temperature increase rate of 5 degrees C per minute for 6 hours, and cooled to room temperature to obtain graphene/carbon coated lithium iron phosphate small-scale nanocomposite. USE - Method for synthesizing graphene/carbon-coated lithium iron phosphate small-scale nanocomposites through aniline polymerization confined effect. ADVANTAGE - The method enables to synthesize graphene/carbon-coated lithium iron phosphate small-scale nanocomposites through aniline polymerization confined effect has good cycle performance.