• 专利标题:   Preparation of graphene nanofilms used in preparation of nano ink, involves immersing cathode and anode comprising graphite foil, in persulfate electrolyte, applying voltage to peel off graphene nanofilms from anode, and separating films.
  • 专利号:   KR2017061121-A, KR1787670-B1
  • 发明人:   HOON L, SUNG O K
  • 专利权人:   MEXPLORER CO LTD
  • 国际专利分类:   B82B003/00, C09D011/52, C25B001/00, C25B011/12
  • 专利详细信息:   KR2017061121-A 02 Jun 2017 C25B-001/00 201751 Pages: 10
  • 申请详细信息:   KR2017061121-A KR065340 26 May 2017
  • 优先权号:   KR180275, KR065340

▎ 摘  要

NOVELTY - Preparation of graphene nanofilms involves immersing a cathode and an anode comprising a graphite foil, in a persulfate electrolyte aqueous solution, applying a positive voltage to the anode and applying a negative voltage to the cathode to peel off the graphene nanofilms from the anode, and separating the graphene nanofilms from the electrolyte. The graphene nanofilms are peeled by performing local oxygen functionalization, such that several gas components are formed by joining an oxygen functional group locally between the edges of the laminated graphite layers. USE - Preparation of graphene nanofilms used in preparation of nano ink (claimed). DETAILED DESCRIPTION - Preparation of graphene nanofilms involves immersing a cathode and an anode comprising a graphite foil, in a persulfate electrolyte aqueous solution, applying a positive voltage to the anode and applying a negative voltage to the cathode to peel off the graphene nanofilms from the graphite layer of the anode, and separating the graphene nanofilms from the electrolyte. The graphene nanofilms are peeled by performing local oxygen functionalization, such that several gas components are formed by joining an oxygen functional group locally between the edges of the laminated graphite layers. During the local oxygen functionalization, hydroxide and oxygen ions are generated at the edges of the graphite layer when water in the aqueous electrolyte solution is electrolyzed, and persulfate ions promote peeling of graphite layer. An INDEPENDENT CLAIM is included for preparation of nano ink, which involves ultrasonically dispersing graphene nanofilms in an organic solvent.