• 专利标题:   Method for preparing titanium dioxide-graphene composite moisture sensitive material, involves dispersing oxidation grapheme, adding ammonia water, heating amorphous titanium dioxide, and separating centrifugal.
  • 专利号:   CN105158295-A
  • 发明人:   CHEN X, LU Y, WANG M, YANG W, ZHAO Y
  • 专利权人:   UNIV BEIJING CHEM TECHNOLOGY
  • 国际专利分类:   G01N027/00
  • 专利详细信息:   CN105158295-A 16 Dec 2015 G01N-027/00 201607 Pages: 9 English
  • 申请详细信息:   CN105158295-A CN10476035 05 Aug 2015
  • 优先权号:   CN10476035

▎ 摘  要

NOVELTY - A titanium dioxide-graphene composite moisture sensitive material preparation method involves dispersing oxidation graphene in ethyl alcohol and oxidation. 25-28 mass% ammonia water is added with oxidation graphene suspension-ethyl alcohol for 10-30 minutes ultrasonic dispersing. Liquid titanium source is slowly added. Amorphous titanium dioxide is heated at 150-180 degrees C under hydrothermal reaction 12-24 hours to obtain graphene. Centrifugal separating process is carried out for 6-12 hours to obtain anatase titanium dioxide-graphene composite material by utilizing freezing and drying sediment. USE - Method for preparing titanium dioxide-graphene composite moisture sensitive material. ADVANTAGE - The method enables preparing titanium dioxide-graphene composite moisture sensitive material with better humidity sensitive property in a simple manner and cost-effective manner without toxicity reagent by utilizing anatase titanium dioxide and grapheme nano composite material and titanium dioxide particle. DETAILED DESCRIPTION - A titanium dioxide-graphene composite moisture sensitive material preparation method involves dispersing oxidation graphene in ethyl alcohol and oxidation to obtain graphene suspension according to 5-10 mg / 100 ml ratio solid/liquid. 25-28 mass% ammonia water is added with oxidation graphene suspension-ethyl alcohol for 10-30 minutes ultrasonic dispersing to obtain suspension-ethyl alcohol according to 1-5/1000 volume ratio ammonia water/oxidation graphite oxide- alkene alcohol suspension. Liquid titanium source is slowly added in dropwise in 400-700 revolutions / minute speed at 20-50 degrees C for 6-24 hours and finally washed by centrifuged to obtain amorphous titanium dioxide-oxidation graphene sediment according to 5-20/1000 volume ratio liquid titanium source/suspension. Amorphous titanium dioxide is heated at 150-180 degrees C under hydrothermal reaction 12-24 hours to obtain graphene. Centrifugal separating process is carried out for 6-12 hours to obtain anatase titanium dioxide-graphene composite material by utilizing freezing and drying sediment.