• 专利标题:   Viscose fiber comprises graphene and viscose cellulose, and is prepared by hydrolyzing corn cob in aqueous solution of inorganic acid, to obtain lignocellulose, and then heating mixture.
  • 专利号:   CN104328523-A, CN104328523-B, WO2016078523-A1, KR2016143817-A, US2017051078-A1, CA2966805-A1, AU2015349249-A1, EP3192902-A1, JP2017521576-W, EP3192902-A4, IN201717016703-A, KR1783951-B1, VN54322-A, JP6253044-B2, MX2017006630-A1, BR112017010591-A2, AU2015349249-B2, RU2017117327-A, CA2966805-C, US10196460-B2, EP3192902-B1, RU2689580-C2
  • 发明人:   GAO S, JIANG C, SUN Z, TANG Y, TIAN W, XU R, ZHANG J, JIANG CH, GAO SH, SUN ZH
  • 专利权人:   JINAN SHENGQUAN GROUP SHARE HOLDING CO L, JINAN SHENGQUAN GROUP CO LTD, JINAN SHENGQUAN GROUP SHARE HOLDING CO L, JINAN SHENGQUAN GROUP SHARE HOLDING CO L, JINAN SHENGQUAN GROUP SHARE HOLDING CO L, JINAN SHENGQUAN GROUP SHARE HOLDING CO L
  • 国际专利分类:   C01B031/04, D01F002/08, C08B009/00, D01F002/10, C01B032/182, D01F002/06, C01B032/184, C01B032/194, C01B032/20
  • 专利详细信息:   CN104328523-A 04 Feb 2015 D01F-002/08 201523 Pages: 6 Chinese
  • 申请详细信息:   CN104328523-A CN10670057 20 Nov 2014
  • 优先权号:   CN10670057, WOCN094290, KR731603, CA2966805

▎ 摘  要

NOVELTY - Viscose fiber comprises 0.05 wt.% graphene and 1.0 wt.% viscose cellulose. USE - Viscose fiber. ADVANTAGE - The viscose fiber has improved breaking strength. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing viscose fiber, which involves: (A) hydrolyzing corn cob in an aqueous solution of an inorganic acid, to obtain lignocellulose; (B) heating the mixture at 70-180 degrees C preferably 100-120 degrees C; (C) adding an acid-sulfite or alkali-sulfite in the mixture, where alkali is selected from calcium hydroxide, sodium hydroxide, ammonium hydroxide or magnesium hydroxide, sufite is selected from calcium sulfite, magnesium sulfite, sodium sulfite or ammonium sulfite, chloride is selected from ferric chloride or ferrous chloride and catalyst is nickel chloride, nickel nitrate, nickel sulfate or nickel acetate; (D) processing the mixture at 50-150 degrees C; and (E) preserving the mixture.