• 专利标题:   Preparation of porous hexagonal cobalt titanate microrod/reduced graphene oxide composite gas-sensitive material involves adding graphene oxide-N-methylpyrrolidone solution to cobalt acetate solution and hydrothermally reacting.
  • 专利号:   CN107935056-A, CN107935056-B
  • 发明人:   LU J, JIA N, XIE L, ZHAO Z, WANG L, LIANG C, MOU Y, MU Y
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY, UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   C01B032/184, C01G051/00, G01N027/00
  • 专利详细信息:   CN107935056-A 20 Apr 2018 C01G-051/00 201842 Pages: 10 Chinese
  • 申请详细信息:   CN107935056-A CN11251001 01 Dec 2017
  • 优先权号:   CN11251001

▎ 摘  要

NOVELTY - Preparation of porous hexagonal cobalt titanate microrod/reduced graphene oxide composite gas-sensitive material involves uniformly dispersing graphene oxide in N-methylpyrrolidone, obtaining graphene oxide solution of N-methylpyrrolidone, dissolving cobalt acetate tetrahydrate and titanium(IV) butoxide in ethylene glycol, stirring at room temperature, adjusting the pH value to 4-6, obtaining light pink solution, adding graphene oxide-N-methylpyrrolidone solution to pale pink solution, ultrasonically stirring at room temperature, adding resultant mixture to a reactor, performing microwave hydrothermal reaction at 180-200 degrees C for 1-3 hours, cooling, washing, drying, and calcining in nitrogen atmosphere. USE - Preparation of porous hexagonal cobalt titanate microrod/reduced graphene oxide composite gas-sensitive material. ADVANTAGE - The method efficiently provides porous hexagonal cobalt titanate microrod/reduced graphene oxide composite gas-sensitive material having excellent sensitivity with respect to ethanol gas, in short period of time at low operating temperature.