• 专利标题:   Preparation of fluorinated graphene with high fluorocarbon ratio for use in preparation of lubricants, involves putting graphene, introducing inert gas, releasing gas to obtain pretreated graphene and carrying out fluorination reaction.
  • 专利号:   CN112624098-A, CN112624098-B
  • 发明人:   XIE Z, XIE X
  • 专利权人:   HUBEI ZHUOXI FLUORINATION CO LTD
  • 国际专利分类:   C01B032/10, C01B032/194
  • 专利详细信息:   CN112624098-A 09 Apr 2021 C01B-032/194 202140 Pages: 7 Chinese
  • 申请详细信息:   CN112624098-A CN10076710 20 Jan 2021
  • 优先权号:   CN10076710

▎ 摘  要

NOVELTY - Preparation of fluorinated graphene with high fluorocarbon ratio, involves Step 1, putting the graphene into the reaction kettle, heating up to 320-350 degrees C, introducing inert gas within 30-60 seconds to increase the pressure to 1-1.5MPa, and maintaining for 1-3 minutes, then releasing the gas, and circulating the above-mentioned pressure-increasing-pressure-holding-pressure reduction steps 5-10 times to obtain pretreated graphene, Step 2, heating the pretreated graphene to 320-350 degrees C and carrying out fluorination reaction. USE - Preparation of fluorinated graphene with high fluorocarbon ratio for use in preparation of lubricants (all claimed). ADVANTAGE - The method increases the fluorine-to-carbon ratio of fluorinated graphene, thereby ensuring good lubricating performance and acid and alkali corrosion resistance.