• 专利标题:   Preparing tin dioxide-graphene composite material useful in lithium ion battery anode material, comprises ultrasonically mixing tin chloride, expanded graphite and organic solvent, subjecting to hydrothermal reaction and centrifugation.
  • 专利号:   CN108649203-A
  • 发明人:   GAO B, WANG W, ZHOU H
  • 专利权人:   ANHUI ANDA NEW ENERGY RESOURCES MATERIAL
  • 国际专利分类:   H01M004/36, H01M004/48, H01M004/62, H01M010/0525
  • 专利详细信息:   CN108649203-A 12 Oct 2018 H01M-004/36 201876 Pages: 6 Chinese
  • 申请详细信息:   CN108649203-A CN10440215 10 May 2018
  • 优先权号:   CN10440215

▎ 摘  要

NOVELTY - Preparing tin dioxide/graphene composite material comprises: (i) mixing large flake graphite, concentrated sulfuric acid and potassium permanganate in a mass ratio of 5:10-15:0.1-0.2 at 40-60 degrees C for 50-60 minutes to obtain expanded graphite; (ii) ultrasonically mixing tin chloride, expanded graphite, organic solvent and water to obtain a precursor solution; (iii) subjecting the precursor solution to microwave high-pressure hydrothermal reaction, centrifugation, filtration, water-washing and drying to obtain a solid powder; and (iv) subjecting the solid powder to first heat treatment at 500-600 degrees C for 10-20 minutes and second heat treatment at 300-350 degrees C for 50-80 minutes. USE - The tin dioxide/graphene composite material is useful in lithium ion battery anode material (claimed). ADVANTAGE - The composite material is simple to prepare and has good electrochemical performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for tin dioxide/graphene composite material.