• 专利标题:   Separating graphene film from liquid graphene-forming matrix involves upon completion of heating/adding hydrocarbon mixture, and during cooling, sliding mould frame over surface of liquid forming matrix, and lifting mould frame above matrix.
  • 专利号:   WO2014035264-A1, WO2014035264-A8, PL400511-A1, EP2888200-A1, PL224447-B1
  • 发明人:   ATRASZKIEWICZ R, DYBOWSKI K, KLINOWSKI B M, KULA P, MODRZYK W, PIETRASIK R, ZAWISTOWSKI P Z
  • 专利权人:   ADVANCED GRAPHENE PROD SP ZOO, ADVANCED GRAPHENE PROD SP ZOO
  • 国际专利分类:   C01B031/04, C30B025/02
  • 专利详细信息:   WO2014035264-A1 06 Mar 2014 C01B-031/04 201420 Pages: 14 English
  • 申请详细信息:   WO2014035264-A1 WOPL000085 11 Sep 2012
  • 优先权号:   PL400511

▎ 摘  要

NOVELTY - Separating graphene film from liquid graphene-forming matrix involves upon completion of process of heating and adding hydrocarbon mixture, and during cooling the forming matrix, in the temperature of 1200-1050 degrees C, and under argon pressure of 10-6 to 1100 hPa, sliding mould frame over surface of liquid forming matrix, where the mould frame contains conductive fibers, during further cooling the mould frame is lowered until contact is achieved with the liquid metal surface of the forming matrix, where after a layer of graphene is attached, mould frame is lifted 1-100 mm above the matrix. USE - For separating graphene film from the liquid graphene-forming matrix (claimed). ADVANTAGE - In the method, the mould or intercepting frame moves vertically at a rate of 0.001-10 mm/second, with the positioning accuracy of 0.001-1 mm. DETAILED DESCRIPTION - A method for separating graphene film from the liquid graphene-forming matrix involves either upon completion of the process of heating and the process of adding a hydrocarbon mixture, and during the cooling the forming matrix, in the temperature of 1200-1050 degrees C, and under argon pressure of 10-6 to 1100 hPa, sliding mould frame over the surface of the liquid forming matrix, where the mould frame consists of conductive fibers, preferably carbon fibers, appropriately stretched and arranged in a characteristic lattice pattern, during further cooling the mould frame is lowered until contact is achieved with the liquid metal surface of the forming matrix, where after a layer of graphene is attached, the mould frame is lifted 1-100 mm above the forming matrix; or upon completion of the process of heating and the process of adding a hydrocarbon mixture, and during the cooling the forming matrix, in the temperature of 1200-1050 degrees C, and under argon pressure of 10-6 to 1100 hPa, operating the intercepting frame together with slidable tape consisting of conductive fibers, preferably carbon fibers, is slid over the surface of the liquid forming matrix, where during further cooling the intercepting frame is lowered until contact is achieved with the liquid metal surface of the forming matrix, where after a layer of graphene is attached, the intercepting frame is lifted 1-100 mm above the forming matrix.