• 专利标题:   Sulfur-magnesium oxide-graphite electrode material useful for lithium-sulfur battery, comprises nano-sulfur electrode material, nano magnesium oxide and graphene.
  • 专利号:   CN107248571-A
  • 发明人:   LIU S, ZHAO S, LIU B
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   H01M010/052, H01M004/36, H01M004/38, H01M004/62
  • 专利详细信息:   CN107248571-A 13 Oct 2017 H01M-004/36 201772 Pages: 6 Chinese
  • 申请详细信息:   CN107248571-A CN10406010 02 Jun 2017
  • 优先权号:   CN10406010

▎ 摘  要

NOVELTY - Sulfur-magnesium oxide-graphite electrode material comprises 45-70 wt.% nano-sulfur electrode material, 3-25 wt.% nano magnesium oxide and graphene (balance). USE - The sulfur-magnesium oxide-graphite electrode material is useful for lithium-sulfur battery. ADVANTAGE - The sulfur-magnesium oxide-graphite electrode material: utilizes cheap raw materials; and has simple preparation technique. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for preparing sulfur-magnesium oxide-graphite electrode material, comprising (1) under argon gas or vacuum condition, heating metal magnesium powder to 700-900 degrees C, and burning with carbon dioxide gas at gas flow rate of 50-100 ml/minute to obtain crude product, (2) adding the crude product based on solid-liquid ratio of 1:6-43 ml into 1-6 M hydrochloric acid solution and magnetic stirring for 1-10 hours, filtering, washing using deionized water until pH reaches to 7-8, then drying to obtain nano magnesium oxide/graphene composite material, and (3) mixing the nano magnesium oxide/graphene composite material and nano-sulfur powder in a molar ratio of 0.4-1.2:1, then subjecting to heat treatment at 130-180 degrees C for 9-15 hours under argon gas atmosphere, and naturally cooling to obtain final product.