• 专利标题:   Preparing low cost and high performance graphene aerogel electrode material comprises e.g. preparing graphene oxide dispersion, mixing graphene oxide dispersion and amine curing agent, and pre-freezing the graphene hydrogel.
  • 专利号:   CN108128769-A
  • 发明人:   ZHANG C
  • 专利权人:   SHANDONG JIAIXNG ENVIRONMENTAL PROTECTIO
  • 国际专利分类:   C01B032/184, C01B032/194, C01B032/198, H01M010/0525, H01M004/587
  • 专利详细信息:   CN108128769-A 08 Jun 2018 C01B-032/184 201841 Pages: 5 Chinese
  • 申请详细信息:   CN108128769-A CN10112797 05 Feb 2018
  • 优先权号:   CN10112797

▎ 摘  要

NOVELTY - Preparing low cost and high performance graphene aerogel electrode material comprises (i) preparing graphene oxide dispersion by stripping graphite oxide method, mixing graphene oxide dispersion and amine curing agent to obtain graphene oxide mixture, where amine curing agent is diaminodiphenylmethane, diaminodiphenyl sulfone, diethylenetriamine and/or triethylenetetramine, (ii) sealing graphene oxide mixed liquid in environment at 90-110 degrees C to heat so that the amine curing agent reduces graphene oxide to obtain graphene hydrogel, and (iii) pre-freezing the graphene hydrogel in vacuum freeze dryer, freezing at -20 degrees C for 45-70 hours to obtain graphene aerogel electrode material. USE - The method is useful for preparing low cost and high performance graphene aerogel electrode material. ADVANTAGE - The method is simple, environmentally friendly, controllable and easy to industrialize; and graphene aerogel is unique and innovative.