• 专利标题:   Preparing non-defective graphene film involves preparing graphene alcohol turbid solution and graphene dispersion, coating turbid solution on substrate, coating dispersion, placing film into kettle for extrusion reaction, rinsing and drying.
  • 专利号:   CN110775963-A
  • 发明人:   YU E
  • 专利权人:   SHAOXING ZIANG NEW MATERIAL CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN110775963-A 11 Feb 2020 C01B-032/184 202017 Pages: 7 Chinese
  • 申请详细信息:   CN110775963-A CN11188909 28 Nov 2019
  • 优先权号:   CN11188909

▎ 摘  要

NOVELTY - Preparing non-defective graphene film involves dispersing graphene powder in anhydrous ethanol and stirring to obtain a graphene alcohol turbid solution. Graphene powder is added to distilled water for ultrasonic dispersion for 20-30 minutes, polyvinyl alcohol is added, and constant temperature ultrasonic dispersion is performed for 20-40 minutes to obtain graphene dispersion. The graphene alcohol turbid solution is uniformly coated on substrate, and dried at constant temperature to obtain graphene base film. The graphene dispersion is coated on surface of base film, and a single graphene film is obtained after constant temperature drying. The single graphene-coated film is inverted, graphene dispersion is applied on surface, and dried at constant temperature. The obtained double-coated graphene film is placed into reaction kettle for constant temperature extrusion reaction for 2-5 hour, cooled, rinsed with distilled water and absolute ethanol, and dried to obtain the desired product. USE - Method for preparing non-defective graphene film. ADVANTAGE - The method solves the defect problem of graphene, and uses the conjugated double bond formed after sintering of polyvinyl alcohol to fill the defect structure of graphene and improves the connection effect of graphene.