• 专利标题:   Preparation of multi-level channel mesoporous graphene/carbon composite material involves synthesizing high-molecular prepolymer, dissolving surfactant with high-molecular prepolymer, carrying out freeze-drying process, and drying.
  • 专利号:   CN103560016-A, CN103560016-B
  • 发明人:   LIU R, LIU S, WAN L, WU D
  • 专利权人:   UNIV SHANGHAI
  • 国际专利分类:   C01B031/02, H01G011/24, H01G011/36, H01M004/1393
  • 专利详细信息:   CN103560016-A 05 Feb 2014 H01G-011/24 201424 Pages: 10 Chinese
  • 申请详细信息:   CN103560016-A CN10480044 11 Oct 2013
  • 优先权号:   CN10480044

▎ 摘  要

NOVELTY - Preparation of multi-level channel mesoporous graphene/carbon composite material involves synthesizing high-molecular prepolymer, dissolving surfactant with the high-molecular prepolymer in which spherical micelle is synthesized, oxidizing the resultant product with graphene, carrying out hydrothermal freeze-drying process at 100 degrees C for 20 hours to obtain graphene aerogel, drying the resultant product under inert atmosphere in which surfactant is removed to obtain multi-level channel mesoporous graphene/carbon composite material. USE - Preparation of multi-level channel mesoporous graphene/carbon composite material used for electric double layer capacitor and lithium battery cathode material. DETAILED DESCRIPTION - Preparation of multi-level channel mesoporous graphene/carbon composite material involves synthesizing high-molecular prepolymer, dissolving surfactant with the high-molecular prepolymer in which spherical micelle is synthesized, oxidizing the resultant product with graphene, carrying out hydrothermal freeze-drying process at 100 degrees C for 20 hours to obtain graphene aerogel, calcining the resultant product, drying under inert atmosphere in which surfactant is removed to obtain multi-level channel mesoporous graphene/carbon composite material. The surfactant is non-ionic surfactant, preferably triblock copolymer. The high-molecular prepolymer is oligomer precursor, preferably phenolic resin prepolymer. The mass ratio of spherical micelle and graphene aerogel is 3:1.